UNIVERSITY OF THE WITWATERSRAND, JOHANNESBURG

Equipment List

Equipment

Use

Location

Contact person

Conditions of Use -Training/Operator

Microscopy and Microanalysis Unit

FEI Spirit 120kV TEM

TEM, STEM, EDX, H DF

Room 1, Biology Building

Mrs Lalkhan
Caroline.Lalkhan@wits.ac.za

User operation, training provided.

JEOL JEM-100S TEM

Basic TEM

Room 1, Biology Building

Mrs Lalkhan
Caroline.Lalkhan@wits.ac.za

User operation, training provided.

Philips 200kV TEM

TEM, STEM, EDX, EELS, H DF

Room 1, Biology Building

Prof Witcomb
Michael.Witcomb@wits.ac.za

Training provided/ operator

JEOL JSM-840 SEM

Basic SEM, BSE

Room 1, Biology Building

Mrs Lalkhan
Caroline.Lalkhan@wits.ac.za

User operation, training provided.

Nova 600 Nanolab FIBSEM

HRSEM, EDX, BSE, micromachining,
3D structure studies, site specific TEM preparation

Room 1, Biology Building

Prof Witcomb
Michael.Witcomb@wits.ac.za

Training provided/ and operator

FEI Quanta 400 ESEM

HRSEM, BSE, EDX, CL, ESEM

Room 1, Biology Building

Mrs Lalkhan
Caroline.Lalkhan@wits.ac.za

User operation, training provided/ and operator

2X Reichert Ultracut E Ultramicrotomes

Sectioning of samples for TEM

Room 1, Biology Building

Mrs Lalkhan
Caroline.Lalkhan@wits.ac.za

User operation, training provided.

Gatan PIPS ion mill

Final thinning of samples for TEM

Room 1, Biology Building

Prof Witcomb
Michael.Witcomb@wits.ac.za

User operation, training provided.

Fischione jet polisher

Final thinning of samples for TEM

Room 1, Biology Building

Prof Witcomb
Michael.Witcomb@wits.ac.za

User operation, training provided.

Two Veeco Atomic Force Microscope instruments

AFM, SPM, many different modes of operation

Room 1, Biology Building

Dr Shrivastava
Sanjiv.Shrivastava@wits.ac.za

Training and operator

Diamond, Thin Hard Films and Related Materials

Locally manufactured specialised equipment for cold cathode emission

With continuous and pulsed HV supply. The system is used to investigate field as well as photon enhanced emissions of materials

Radiation and Health Physics Unit

T. Nam
Tom.Nam@wits.ac.za

Due to its heavy use by the group and it is still under development the system at this point in time is not available to outside users.

Lenton TSH 12/38/250 tube furnace

Sample heating under different atmosphere

Radiation and Health Physics Unit

T. Nam
Tom.Nam@wits.ac.za

Available for use

Senographe 500t mammography unit

Used for low energy X-ray detector development

Radiation and Health Physics Unit

T. Nam
Tom.Nam@wits.ac.za

Available for use by registered radiation worker

PTW Unidose E

For checking and calibrating radiation responses of detectors

Radiation and Health Physics Unit

T. Nam
Tom.Nam@wits.ac.za

Available for use

Well Diamond Wire Saw

Precision slicing of samples

Physics mezzanine

C. Levitt or T. Derry
Trevor.Derry@wits.ac.za

Training

Ion implantion facilities at iThemba LABS (Gauteng)

Surface modification, thin layer doping, radiation damage, etc.

Former Schonland Res. Inst, Empire Rd.

Trevor Derry, Mervin Naidoo Trevor.Derry@wits.ac.za

Operated by former, by special agreement

Optical Spectroscopy Laboratory

High resolution optical spectroscopy Jarrell-Ash 1m double grating spectrograph fitted with a G s photomultiplier and photon counting electronics.

Low temperature (77 K ? 8 K) fluorescence studies of doped crystalline samples. Suitable for dopants that show absorption in the 635 ? 660 nm region.

P20, Physics building

Marjorie Mujaji
P201, Physics building
X76846

Training

Strong Metallic Alloys - Mintek

Vacuum and air induction furnaces

Melting & Casting

Mintek

Chris Fletcher
chrisf@mintek.co.za

Technician/instrument scientist will always run the samples

Water atomiser

Powder manufacture, base and precious metals

Alain Mwamba
Alainm@mintek.co.za

80 tonne uniaxial compaction press

Consolidation of powders

Alain Mwamba

Fabrication - forging, hot/cold rolling, etc.

Sample shaping

Chris Fletcher

Air muffle furnaces, vacuum tube and sintering furnaces

Heat treatment different temperatures up to 1800C)

Chris Fletcher

Fatigue, tensile, 3 point bend rigs, hardness testers (Brinell and Vickers)

Mechanical testing:

Chris Fletcher

Metallography Lab with optical microscopes

Sample prep (grinding, polishing, etching)

Mintek

Alain Mwamba

Basic operation can be taught

Image analysis software

Alain Mwamba

technician/instrument scientist will always run the samples

  • Potensiostats
  • Autoclaves (can be set up for HIC testing, only Lab in SA)
  • Stress Corrosion

Corrosion testing

Lesley Chown
Lesley@mintek.co.za

High Resolution NanoNova SEM with EDS (incl. mapping) and EBSD

Imaging, chemical analysis, crystal structure

Lesley Chown

NETZSCH Simultaneous Thermal Analysis Facility (DTA TGA DSC)

Thermal analysis, thermogravimetry, calorimetry of metals


Lesley Chown

SIEMENS XRD

Crystal structure, rest-austenite

Lesley Chown

Vacutec EB-PVD

Thin films and coatings

Lesley Chown

Thermo-CalcTM Laptop

Databases:

  • Fe, Al, Mg databases
  • Building Pt based alloy database

Prediction of phase diagrams, phase equilibria, liquidus temperatures

Lesley Chown

Access provided to trained people

Strong Metallic Alloys ? Wits

Software:

  • JEMS software

simulation of TEM images and diffraction patterns

Physics

K. Pruessner

contact(011)717-6821

  • Thermo-Calc steels database ( used for 4th year students 2008?

Prediction of phase diagrams, phase equilibria, liquidus temperaratures

Richard Ward

L. Cornish
Lesley.Cornish@wits.ac.za

Access provided to trained people

  • Crystal Diffract software

Richard Ward

L. Cornish
Lesley.Cornish@wits.ac.za

Access provided to trained people

New Ultrahard materials - Computational Physics Cluster

Hardware

multi-core (P4 to Xenon): 70 nodes.

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

fast GHz 48 port switch

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

System Software

Linux (Intel compilers)

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

Specialised Software

Vasp, Fhi, Espresso, Abinit

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

Siesta, Aimpro, Gammes

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

Dlpoly, Gulp, Moldy, Xmd

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

Visualization

Vesta, Diamond,

Physics building

Ted Lowther
John.Lowther@wits.ac.za

Access provided to trained people

Carbon Nanotubes and Strong Composites

TGA

Used for evaluating temperature effects on a material e.g. weight loss under air or nitrogen.

Gate House 8th Floor

Messai Mamo
Edward Nxumalo
Mahluli Moyo

If significant use expected ? student will be trained in use

TPR

Used for analysing the reduction behaviour of metal oxides. Equipment also permits measurement of gas desorption.

Room 114 , Chemistry

Thabiso Phadi
Basil Chassoulas

If significant use expected ? student will be trained in use

Magnetic Resonance Laboratory
X- band Electron Magnetic Resonance spectrometer (continuous wave and FT-EMR) Characterization of materials and fundemental physics studies Room P27,
Physics Building
Jonathan Keartland
Jonathan.keartland@wits.ac.za
Trained users are welcome to utilize the equipment

Pulsed broad-line Nuclear Magnetic Resonance spectrometer

Characterization of materials and fundamental physics studies

Room P27, Physics Building

Johathan Keartland
Jonathan.keartland@wits.ac.za

Use restricted to students and staff of the laboratory

Corrosion facilities

Potentiostats

  • Autolab

Corrosion rates; corrosion charaterisation

Richard Ward Room 403

Josias van der Merwe
Josias.vandermerwe@wits.ac.za

Training and operator

  • Potentio-dynamic testing: DC as well as AC

Corrosion interface analyses; Coating corrosion resistance characterisation

Richard Ward Room 403

Josias van der Merwe

Training and operator

  • Solartron , Software on order

Corrosion rates; corrosion charaterisation; Corrosion interface analyses; Coating corrosion resistance characterisation

Richard Ward Room 403

Josias van der Merwe

Training and operator

Ultrasonic cleaning

Sample cleaning

Richard Ward Room 403

Josias van der Merwe

None

Autoclave High temperature and high pressure exposure tests, Influence of flow rate, SCC constant deformation, C-ring, U-bend specimens, Weight loss tests

Corrosion rate determination at high temperatures and pressures for stagnant and turbulent conditions

Richard Ward Room 403

Josias van der Merwe

Training

Salt spray cabinet

Atmospheric evaluation of coatings

Richard Ward Room 403

Josias van der Merwe

Operator